Preparation of monodisperse carbon nanospheres for electrochemical capacitors

The efficiently hydrothermal route using sucrose without any catalysts is employed to prepare the uniform carbon spheres. The monodisperse 100–150 nm carbon spheres are obtained with the activation treatment in molten KOH. The carbon spheres are characterized by transmission electron microscope, X-ray diffraction, N₂ adsorption, Raman spectroscopy and electrochemical techniques. The relationships of specific capacitance and surface properties of carbon spheres are investigated. A single electrode of carbon nanosphere materials performs excellent specific capacitance (328 F g^?1), area capacitance (19.2 μF cm^?2) and volumetric capacitance (383 F cm^?3).