Synthesis, characterization, and structural study of K2FeZrP3O12 with the langbeinite structure |
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| Authors: | Albina I Orlova Victoria S Kurazhkovskaya Miguel A Salvadó Sergei A Khainakov |
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| Institution: | a Department of Chemistry, Nizhni Novgorod State University, pr. Gagarina 23, Nizhni Novgorod 603950, Russiab Department of Geology, Moscow State University, Vorob’evy gory, Moscow 119899, Russiac Departamento de Qu?́mica F?́sica y Anal?́tica, Universidad de Oviedo, Oviedo 33006, Spaind Departamento de Qu?́mica Orgánica e Inorgánica, Facultad de Quimica, Universidad de Oviedo, Oviedo 33006, Spain |
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| Abstract: | A potassium iron zirconium phosphate, K2FeZrP3O12, was synthesized by thermal treatment of a material obtained by the sol-gel method, mixing two aqueous solutions, the first containing KCl, FeCl3 and ZrOCl2, and the second, H3PO4. The crystal structure was refined using powder X-ray diffraction data. The unit cell is cubic, a=10.0554(3) Å, space group P213. This compound is the first iron zirconium phosphate described with a langbeinite-type structure. |
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