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| 4-二甲氨基吡啶催化合成含氟苯甲酸糖酯 | |
| 引用本文： | 陈洪,符史良,徐亚平,黄筱玲.4-二甲氨基吡啶催化合成含氟苯甲酸糖酯[J].合成化学,2002,10(3):274-276. |
| 作者姓名： | 陈洪 符史良 徐亚平 黄筱玲 |
| 作者单位： | 1. 湛江海洋大学,广东,湛江,524088 2. 井冈山师范学院,江西,吉安,343009 3. 武汉大学,湖北,武汉,430072 |
| 摘 要： | 以4－二甲氨基吡啶为催化剂由含氟苯甲酸与溴代乙酰糖催化酯化合成了4个新的含氟苯甲酸糖酯。其结构经IR，^1H NMR和MS确认，多数还作了^13C NMR测定。 |
| 关 键 词： | 催化合成 4－二甲氨基吡啶 糖酯 含氟苯甲酸 催化剂 结构 农药 抗植物病毒活性 |
| 文章编号： | 1005-1511(2002)03-274-03 |
| 修稿时间： | 2001年9月20日 |
Synthesis of Fluoro-containing Saccharide Carboxylate Catalyzed by 4-Dimethylaminepyridine |
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| CHEN Hong ,FU Shi-liang ,XU Ya-ping ,HUANG Xiao-ling.Synthesis of Fluoro-containing Saccharide Carboxylate Catalyzed by 4-Dimethylaminepyridine[J].Chinese Journal of Synthetic Chemistry,2002,10(3):274-276. | |
| Authors: | CHEN Hong FU Shi-liang XU Ya-ping HUANG Xiao-ling |
| Institution: | CHEN Hong 1,FU Shi-liang 1,XU Ya-ping 2,HUANG Xiao-ling 3 |
| Abstract: | Four new fluoro-containing saccharide carboxylates from fluoro-containing benzoin acids and o-acetylglucopyranosyl bromide or o-acetylgalactopyranosyl bromide were synthesized in the presence of 4-dimethylaminepyridine and their structres were confirmed by elemental analysis, IR, 1H NMR and 13C NMR. |
| Keywords: | dimethylaminepyridine catalysis saccharide carboxylate synthesis fluoro-containing benzoic acid |
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