双峰倍增配平导数—同步荧光法同时测定苯酚和间苯二酚的研究 |
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引用本文: | 唐波 何锡文. 双峰倍增配平导数—同步荧光法同时测定苯酚和间苯二酚的研究[J]. 分析试验室, 1997, 16(3): 18-22 |
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作者姓名: | 唐波 何锡文 |
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作者单位: | 山东师范大学化学系,南开大学化学系 |
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基金项目: | 山东省青年自然科学基金,国家教育委员会博士点基金 |
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摘 要: | 本文提出用双峰倍增配平法计算解析苯酚和间苯二酚混合体系的一阶导数-同步荧光光谱,测定结果的回收率,精密度和两组分间浓度比范围均统一阶导数-同步荧光法优方法用于雷琐辛涂剂和水样中苯酚与间苯二酚的测定,结果令人满意。
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关 键 词: | 双峰倍增配平 苯酚 间苯二酚 同步荧光 导数技术 |
Study on Simultaneous Determination of Phenol and Resorcinol Using Dual Peak Multiplication Balance Derivative Synchronous Fluorimetry |
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Abstract: | In this paper ,the computational analysis of the first order derivative synchronous fluorescence spectra of phenol and resorcinol by dual peak multiplication balance has been proposed,this method has the advantages over the analysis of fluorescence spectra of phenol and resorcinol by first order derivative synchronous technique in terms of precision,recovery and range of concentration ratio of the two components in a mixture.The proposed method has been used to determine phenol and resorcinol in pharmaceutical preparations and water samples with satisfactory results. |
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Keywords: | Dual peak multiplication balance phenol resorcinol synchronous fluorimetry derivative technique |
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