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Ce掺杂In_2O_3纳米纤维的制备及其三乙胺气敏性能(英文)
引用本文:王金兴,于连香,王浩铭,李圣平,李佳静,吴凤清.Ce掺杂In_2O_3纳米纤维的制备及其三乙胺气敏性能(英文)[J].物理化学学报,2010,26(11):3101-3105.
作者姓名:王金兴  于连香  王浩铭  李圣平  李佳静  吴凤清
作者单位:1. College of Chemistry, Jilin University, Changchun 130012, P. R. China; 2. Changchun Institute of Automobile Materials, Changchun 130011, P. R. China; 3. College of Electronic Science and Engineering, Jilin University, Changchun 130012, P. R. China
基金项目:the National Natural Science Foundation of China,Jilin Provincial Science and Technology Department,Seed Foundations of Jilin University;China,National High-Tech Research and Development Program of China(863),Doctoral Found of Ministry of Education of China,国家自然科学基金,吉林省科技基金,吉林大学种子基金,国家高技术研究发展计划项目(863),教育部博士点基金
摘    要:用简单有效的静电纺丝法制备了Ce掺杂的In2O3纳米纤维材料.采用X射线衍射(XRD)、透射电子显微镜(TEM)、高分辨率透射电子显微镜(HRTEM)和扫描电子显微镜(SEM)对合成样品的晶体结构和形貌进行了表征.结果显示,此纤维材料的平均直径约为90nm,长度达到几十个微米.气敏性能测试结果表明,4%(w)Ce掺杂的In2O3纳米纤维对三乙胺的灵敏度最高,该气敏元件对3μL·L-1三乙胺的灵敏度达到2.6,响应时间为5s,恢复时间约为6s,且具有较好的选择性.

关 键 词:静电纺丝法  Ce  掺杂In2O3  纳米纤维  三乙胺  气体传感器  
收稿时间:2010-05-11
修稿时间:2010-10-09

Preparation and Triethylamine Sensing Properties of Ce-Doped In2O3 Nanofibers
WANG Jin-Xing,YU Lian-Xiang,WANG Hao-Ming,RUAN Sheng-Ping,LI Jia-Jing,WU Feng-Qing.Preparation and Triethylamine Sensing Properties of Ce-Doped In2O3 Nanofibers[J].Acta Physico-Chimica Sinica,2010,26(11):3101-3105.
Authors:WANG Jin-Xing  YU Lian-Xiang  WANG Hao-Ming  RUAN Sheng-Ping  LI Jia-Jing  WU Feng-Qing
Institution:1. College of Chemistry, Jilin University, Changchun 130012, P. R. China; 2. Changchun Institute of Automobile Materials, Changchun 130011, P. R. China; 3. College of Electronic Science and Engineering, Jilin University, Changchun 130012, P. R. China
Abstract:Ce-doped In2O3 nanofibers were synthesized by a simple and effective electrospinning method. The morphology and crystal structure of the as-prepared samples were characterized by X-ray diffraction (XRD),transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), and scanning electron microscopy (SEM). The results revealed that the length of the nanofibers can reach several tens of micrometers and the average diameter was about 90 nm. The sensor fabricated from the 4% (w) Ce-doped In2O3 nanofibers showed the highest sensitivity to triethylamine. The sensitivity reached 2.6 when the sensor was exposed to 3 μL·L-1 triethylamine and the response time and recovery time were about 5 and 6 s, respectively. Moreover, good selectivity was also observed in our investigation.
Keywords:Electrospinning method  Ce-doped In2O3  Nanofibers  riethylamine  Gas sensor
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