| o-ZrW1.6Mo0.4O8·H2O正交相的合成与表征 |
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| 引用本文： | 黄令,刘鹏辉,马辉,齐传民,赵新华.o-ZrW1.6Mo0.4O8·H2O正交相的合成与表征[J].无机化学学报,2005,21(10):1531-1534. |
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| 作者姓名： | 黄令 刘鹏辉 马辉 齐传民 赵新华 |
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| 作者单位： | 1. 北京师范大学化学系,北京,100875
2. 北京师范大学分析测试中心,北京,100875 |
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| 基金项目： | 国家自然科学基金(No.20471010,20371009)，北京市无机化学重点学科项目资助 |
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| 摘 要： | The precursor ZrW1.6Mo0.4O7(OH)2(H2O)2 was characterized by IR and XRD methods. δ′-ZrW1.6Mo0.4O8 was prepared by careful controlling the annealing conditions from the precursor and was determined to have the formula as o-ZrW1.6Mo0.4O8·H2O by TG-DSC, IR, and XRD methods. The relation between o-ZrW1.6Mo0.4O8·H2O and o-ZrW1.6Mo0.4O8 was discussed through variable temperature XRD patterns. Further more, the mechanism of the precursor dehydration was suggested.
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| 关 键 词： | ZrW1.6Mo0.4O8·H2O 合成 表征 |
| 文章编号： | 1001-4861(2005)10-1531-04 |
| 收稿时间： | 3/6/2005 12:00:00 AM |
| 修稿时间： | 2005年3月6日 |
The Preparation and Characterization of Orthorhombic o-ZrW1.6Mo0.4O8· H2O |
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| HUANG Ling,LIU Peng-Hui,MA Hui,QI Chuan-Min and ZHAO Xin-Hua.The Preparation and Characterization of Orthorhombic o-ZrW1.6Mo0.4O8· H2O[J].Chinese Journal of Inorganic Chemistry,2005,21(10):1531-1534. |
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| Authors: | HUANG Ling LIU Peng-Hui MA Hui QI Chuan-Min and ZHAO Xin-Hua |
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| Institution: | Department of Chemistry, Beijing 100875,Department of Chemistry, Beijing 100875,Analyzing and Testing Center, Beijing Normal University, Beijing 100875,Department of Chemistry, Beijing 100875 and Department of Chemistry, Beijing 100875 |
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