Complete Assignment of the 1H and 13C NMR Spectra of Carthamin Potassium Salt Isolated from Carthamus tinctorius L. |
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Authors: | Maiko Sasaki Keiko Takahashi |
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Institution: | Faculty of Engineering, Tokyo Polytechnic University, 1583, Iiyma Atsugi, Kanagawa 243-027, Japan; |
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Abstract: | Carthamin potassium salt isolated from Carthamus tinctorius L. was purified by an improved traditional Japanese method, without using column chromatography. The 1H and 13C nuclear magnetic resonance (NMR) signals of the pure product were fully assigned using one- and two-dimensional NMR spectroscopy, while the high purity of the potassium salt and deprotonation at the 3′ position of carthamin were confirmed by atomic adsorption spectroscopy and nano-electrospray ionization mass spectrometry. |
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Keywords: | carthamin-3′ potassium salt green metallic luster fermented safflower petal tablet |
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