Crystal Structure of 6,6′-dimethoxy-2,2′-diphenyl-19-crown-5 Hg(SCN)2 |
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Authors: | L. E. Ochando J. M. Amigo A. M. Costero M. Pitarch T. Debaerdemaeker |
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Abstract: | The crystal structure of 6,6′-dimethoxy-2,2′-diphenyl-19-crown-5 Hg(SCN)2 has been determined from three-dimensional X-ray diffraction data. The compound crystallizes in the triclinic space group P1 (no 2) with unit cell parameters α = 9.712(6) Å, β = 11.137(7) Å, c = 14.768(12) Å, α = 86.04(5), β = 80.36(4), γ = 65.70(4), Z = 2, V= 1435(2) Å3. The structure was determined by direct methods which on refinement yielded a final value of R(F) index as 0.068. |
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