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溶剂热法制备Bi2S3纳米材料
引用本文:袁爱华,汪萍,潘励,周虎,马卉. 溶剂热法制备Bi2S3纳米材料[J]. 无机化学学报, 2006, 22(3): 559-562
作者姓名:袁爱华  汪萍  潘励  周虎  马卉
作者单位:1. 江苏科技大学材料科学与工程学院,镇江,212003
2. 江苏大学材料科学与工程学院,镇江,212013
基金项目:江苏省教育厅自然科学基金
摘    要:0引言纳米材料具有特殊的结构和性能,可广泛应用于化学、物理学、电子学、光学、机械和生物医药学等领域[1 ̄5]。其中一维或准一维纳米结构体系或纳米材料的研究既是研究其它低维材料的基础,又与纳米电子器件及微型传感器密切相关,是近年来国内外研究的前沿[6 ̄9]。近年来,人们虽然做了许多尝试来制备一维纳米结构材料,但合成这类材料特别是合成半导体一维纳米材料仍然是一个巨大的挑战。随着维数的减小,半导体材料的电子能态发生变化,其光、电、声、磁等方面性能与常规体材料相比有着显著的不同[10 ̄12]。Bi2S3是一种重要的半导体材料,受…

关 键 词:溶剂热法; Bi2S3; 纳米材料
文章编号:1001-4861(2006)03-0559-04
收稿时间:2005-09-19
修稿时间:2005-12-06

Bi2S3 Nanoflowers and Nanorods Synthesized by Solvothermal Method
YUAN Ai-Hu,WANG Ping,PANG Li,ZHOU Hu and MA Hui. Bi2S3 Nanoflowers and Nanorods Synthesized by Solvothermal Method[J]. Chinese Journal of Inorganic Chemistry, 2006, 22(3): 559-562
Authors:YUAN Ai-Hu  WANG Ping  PANG Li  ZHOU Hu  MA Hui
Affiliation:School of Material Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang, Jiangsu 212003,School of Material Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang, Jiangsu 212003,School of Material Science and Engineering, Jiangsu University, Zhenjiang, Jiangsu 212013,School of Material Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang, Jiangsu 212003 and School of Material Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang, Jiangsu 212003
Abstract:By using Bi(S2CNEt2)3 as single-source precursor, Bi2S3 nanoflowers and nanorods have been obtained via a solvothermal treatment. The effect of water, ethylene glycol and polyethylene glycol as reaction medium on the structure and shape of Bi2S3 nanosized materials was investigated, and Bi2S3 nanoflowers and nanorods were characterized by SEM, TEM and XRD.
Keywords:solvothermal treatment   Bi2S3   nanosized materials
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