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Synthesis of New Glyoxime Derivatives,Characterization and Investigation of Their Complexes with Co(II), Ni(II), and Cu(II) Metals and Thermal Studies
Authors:E. G. Ozkan  E. Canpolat  M. Kaya
Affiliation:(1) Department of Chemistry, Faculty of Arts and Sciences, University of Firat, Elazig, Turkey
Abstract:
In this study, two new vic-dioxime ligands and their complexes with Co2+, Ni2+, and Cu2+ ions were synthesized. Secondary amines (morpholine and piperidine) reacted with anti-chloroglyoxime to give morpholineglyoxime (H2L1) and piperidineglyoxime (H2L2) ligands. All the complexes have a metal to ligand ratio of 1 : 2. The structure of the ligands and their complexes was proposed from elemental analyses, IR, UV-VIS, 1H and 13C NMR spectra, conductivity, magnetic susceptibility measurements, and thermogravimetric analyses.__________From Koordinatsionnaya Khimiya, Vol. 31, No. 7, 2005, pp. 535–539.Original English Text Copyright © 2005 by Ozkan, Canpolat, Kaya.The text was submitted by the authors in English.
Keywords:
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