| 季戊四醇螺环磷酸苯酚酯的合成及结构表征 |
| |
| 引用本文： | 孙才英,李斌,张转芳,邵博,徐树财.季戊四醇螺环磷酸苯酚酯的合成及结构表征[J].应用化学,2006,23(2):165-0. |
| |
| 作者姓名： | 孙才英 李斌 张转芳 邵博 徐树财 |
| |
| 作者单位： | 东北林业大学化学化工系 |
| |
| 基金项目： | 国家自然科学基金;东北林业大学校科研和教改项目 |
| |
| 摘 要： | 季戊四醇螺环磷酸苯酚酯的合成及结构表征;季戊四醇螺环磷酸苯酚酯;季戊四醇螺环磷酰二氯;苯酚;绿色合成
|
| 关 键 词： | 季戊四醇螺环磷酸苯酚酯的合成及结构表征 季戊四醇螺环磷酸苯酚酯 季戊四醇螺环磷酰二氯 苯酚 绿色合成 |
| 文章编号： | 1000-0518(2006)02-0165-04 |
| 收稿时间： | 2005-04-08 |
| 修稿时间： | 2005-08-02 |
Synthesis and Characterization of Bis-phenol Ester of Spirocylic Pentaerythritol Bis-chlorophosphatidic Acid |
| |
| SUN Cai-Ying,LI Bin,ZHANG Zhuan-Fang,SHAO Bo,XU Shu-Cai.Synthesis and Characterization of Bis-phenol Ester of Spirocylic Pentaerythritol Bis-chlorophosphatidic Acid[J].Chinese Journal of Applied Chemistry,2006,23(2):165-0. |
| |
| Authors: | SUN Cai-Ying LI Bin ZHANG Zhuan-Fang SHAO Bo XU Shu-Cai |
| |
| Institution: | Department of Chemistry, University of Northeast Forestry,Harbin 150040 |
| |
| Abstract: | With water as solvent, the bis-phenol ester of spirocylic pentaerythritol bis-chlorophosphatidic acid was prepared from spirocyclie pentaerythritol bis-chlorophosphatide and phenol under alkaline condition. The reaction time was determined by monitering the reaction process with the absorbency variation of phenol sodium in the reaction system at 269. 6 nm. The product structure was characterized with FTIR, ^1H NMR and the phosphorus amount. The thermal stability of the product was analysed with TG measurement. |
| |
| Keywords: | bis-phenol ester of spirocylic pentaerythfitol bis-chlorophosphatidic acid spirocyclie pentaerythritol bis-chlorophosphatide phenol |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
| 点击此处可从《应用化学》浏览原始摘要信息 |
| 点击此处可从《应用化学》下载免费的PDF全文 |
