| 甲基二甲氧基硅烷的合成 |
| |
| 引用本文： | 余淑娴,邓仲明,曾纪术,彭勇,李小林,陈其阳,廖洪流,范宏芳,胡音莉.甲基二甲氧基硅烷的合成[J].南昌大学学报(理科版),2003,27(3):263-266. |
| |
| 作者姓名： | 余淑娴 邓仲明 曾纪术 彭勇 李小林 陈其阳 廖洪流 范宏芳 胡音莉 |
| |
| 作者单位： | 1. 南昌大学,化材学院,江西,南昌,330047
2. 星火化工厂,星辰实验室,江西,永修,330319 |
| |
| 摘 要： | 介绍了由CH3SiHC12和CH3OH进行酯化反应，采用混合溶剂法制备甲基二CH3(OCH3)2SiH]，研究了不同溶剂和反应条件对醇解反应的影响，对反应产物进行GC-MS，IR定性定量分析，同时确定了较优的合成条件。
|
| 关 键 词： | 甲基二甲氧基硅烷 合成 甲基二氯硅烷 甲醇 酯化反应 混合溶剂法 |
| 文章编号： | 1006-0464(2003)03-0263-04 |
| 修稿时间： | 2002年12月4日 |
THE PREPARATION OF METHYLDIMETHOXYSILANE |
| |
| YU Shu-xian,DENG Zhong-ming,ZENG Ji-shu,PENG Yong,LI Xiao-lin,CHENG Qi-yang,LIAO Hong-liu,FAN Hong-fang,HU Yin-li.THE PREPARATION OF METHYLDIMETHOXYSILANE[J].Journal of Nanchang University(Natural Science),2003,27(3):263-266. |
| |
| Authors: | YU Shu-xian DENG Zhong-ming ZENG Ji-shu PENG Yong LI Xiao-lin CHENG Qi-yang LIAO Hong-liu FAN Hong-fang HU Yin-li |
| |
| Institution: | YU Shu-xian~1,DENG Zhong-ming~1,ZENG Ji-shu~1,PENG Yong~1,LI Xiao-lin~1,CHENG Qi-yang~2,LIAO Hong-liu~2,FAN Hong-fang~2,HU Yin-li~2 |
| |
| Abstract: | Methyldimethoxysilane was synthesized by the esterification reaction of Methyldichlorosilane and Methanol in mixed inert solvents. The effects of different solvents and reaction conditions on the alcoholysis were studied. The composition of products were examined by IR and GC-MS method. And the appropriate reaction conditions were established. |
| |
| Keywords: | methyldimethoxysilane methyldichlorosilane methanol synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
