| 多相催化反应原位红外系统及其应用 |
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| 引用本文： | 季生福,李树本,寇元,张兵,牛建中,赵鑫淼.多相催化反应原位红外系统及其应用[J].分析测试技术与仪器,1997,3(4):204-209. |
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| 作者姓名： | 季生福 李树本 寇元 张兵 牛建中 赵鑫淼 |
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| 作者单位： | 中国科学院兰州化学物理研究所羰基合成与选择氧化国家重点实验室 |
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| 基金项目： | 国家基金委重大基金,中国科学院计划财务局大型仪器功能开发基金 |
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| 摘 要： | 设计和建立了一套能耐高温的用于多相催化反应研究的原位红外系统，反应温度从室温到１１５０Ｋ，系统真空为１．０＊１０＾５－１．０－１０＾－４Ｐａ，红外光谱检测范围为４８００－２００ｃｍ＾－１。此系统扩展了原仪器的功能，提高了仪器利用率和效率。
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| 关 键 词： | 多相催化反应 原位红外系统 红外光谱法 |
| 收稿时间： | 1997/9/24 0:00:00 |
| 修稿时间： | 1997/11/24 0:00:00 |
Design and Application of an in situ FTIR System for Heterogeneous Catalytic Reaction |
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| Ji Shengfu,Li Shuben,Kou Yuan,Zhang Bin,Niu Jianzhong and Zhao Xinmiao.Design and Application of an in situ FTIR System for Heterogeneous Catalytic Reaction[J].Analysis and Testing Technology and Instruments,1997,3(4):204-209. |
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| Authors: | Ji Shengfu Li Shuben Kou Yuan Zhang Bin Niu Jianzhong and Zhao Xinmiao |
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| Institution: | State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000;State Key Laboratory for Oxo Synthesis and Selective Oxidation, Lanzhou Institute of Chemical Physics, the Chinese Academy of Sciences Lanzhou 730000 |
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| Abstract: | An in situ FTIR system which can endure hig hreaction temperature for heterogeneous catalytic reaction is desigened and set up. The reaction temperature of the systemform can be from room temperature to 1 150 K,with vacuum from 1.0×105Pa to 1.0×10-4 Pa, and the IR spectral range is 4800cm-1 to 200cm-1. The sample can be easily loaded. The function of the Bruker IFS 120HR FTIR spectrometer is extended and the efficiency of the measurement was also improved. |
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| Keywords: | heterogeneous catalytic reaction in situ FTIR system |
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