| 3,6-二甲基-9-芳基-2,7-二氧杂-1,2,7,8,9,10-六氢-1,8-吖啶二酮衍生物的一步合成 |
| |
| 引用本文： | 刘波,李卓宁,张雪利,吕维中,高原. 3,6-二甲基-9-芳基-2,7-二氧杂-1,2,7,8,9,10-六氢-1,8-吖啶二酮衍生物的一步合成[J]. 有机化学, 2008, 28(6): 1071-1073 |
| |
| 作者姓名： | 刘波 李卓宁 张雪利 吕维中 高原 |
| |
| 作者单位： | 深圳大学化学化工学院,深圳,518060 |
| |
| 摘 要： | 以芳醛、6-甲基-4-羟基-2-吡喃酮、醋酸铵为原料, 醋酸为溶剂, 一步合成了一系列3,6-二甲基-9-芳基-2,7-二氧 杂-1,2,7,8,9,10-六氢-1,8-吖啶二酮, 产物的结构经红外、核磁、元素分析进行了表征, 并对反应过程提出了可能的机理.
|
| 关 键 词： | 芳醛 6-甲基-4-羟基-2-吡喃酮 吖啶二酮 |
| 收稿时间： | 2006-12-05 |
| 修稿时间： | 2006-01-25 |
One-Pot Synthesis of 9-Aryl-3,6-dimethyl-2,7-dioxa-1,2,7,8,9,10- hexahydro-1,8-acridinedione Derivatives |
| |
| LIU,Bo,LI,Zhuo-Ning,ZHANG,Xue-Li,L,Wei-Zhong,GAO,Yuan. One-Pot Synthesis of 9-Aryl-3,6-dimethyl-2,7-dioxa-1,2,7,8,9,10- hexahydro-1,8-acridinedione Derivatives[J]. Chinese Journal of Organic Chemistry, 2008, 28(6): 1071-1073 |
| |
| Authors: | LIU Bo LI Zhuo-Ning ZHANG Xue-Li L Wei-Zhong GAO Yuan |
| |
| Affiliation: | (College of Chemistry and Chemical Engineering, Shenzhen University, Shenzhen 518060) |
| |
| Abstract: | A series of 9-aryl-3,6-dimethyl-2,7-dioxa-1,2,7,8,9,10-hexahydro-1,8-acridinedione derivatives were synthesized by one-pot reaction of substituted benzaldehyde, 4-hydroxyl-6-methyl-2-pyranone with ammonium acetate in acetic acid. The structures of the products were determined by IR, 1H NMR spectra and elemental analysis. A possible mechanism for this reaction was proposed. |
| |
| Keywords: | aromatic aldehyde 4-hydroxyl-6-methyl-2-pyranone acridinedione |
| 本文献已被 维普 万方数据 等数据库收录！ |
| 点击此处可从《有机化学》浏览原始摘要信息 |
|
点击此处可从《有机化学》下载全文 |
|
