Integrated approaches for reducing sample size for measurements of trace elemental impurities in plutonium by ICP-OES and ICP-MS |
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Authors: | Ning Xu Rebecca M Chamberlin Pam Thompson Philip Kaye |
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Institution: | 1.School of Materials Science and Engineering,Southwest University of Science and Technology,Mianyang,China;2.Engineering Research Center of Biomass Materials,Ministry of Education,Mianyang,China |
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Abstract: | A novel microsphere adsorbent based upon carboxymethyl cellulose sodium/prussian blue composite loaded with Lanthanum(III) (CMC/PB-La) was successfully synthesized via electrostatic ejection device for removal of cesium from contaminated water, and characterized by FT-IR, SEM, EDX and XPS. Influencing factors to adsorption cesium were investigated, including solution pH, adsorbent dosage, contact time, initial concentration, temperature and competing ions. Linear Freundlich isotherm was fitted satisfactorily to the adsorption data, and the adsorption kinetic data was fitted well with pseudo-second-order model. Moreover, the results of γ-irradiation experiments indicate that CMC/PB-La has good radiation stability. |
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