| 微波消解-ICP-AES测定海鸭蛋中的金属元素 |
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| 引用本文： | 罗虎,邓全道,许光,梁德荣. 微波消解-ICP-AES测定海鸭蛋中的金属元素[J]. 光谱实验室, 2012, 29(1): 314-316 |
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| 作者姓名： | 罗虎 邓全道 许光 梁德荣 |
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| 作者单位： | 1. 钦州出入境检验检疫局 535000
2. 中国检验认证集团广西有限公司钦州分公司 535000 |
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| 摘 要： | 建立微波消解海鸭蛋,电感耦合等离子体-原子发射光谱法检测样品中金属元素的方法。分析结果表明,15种元素的相对标准偏差(RSD,n=12)小于2%,回收率范围在91.0%-105.4%之间。该法快速,简单,可靠性高,可多元素同时测定,适用于海鸭蛋的快速分析检测。
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| 关 键 词： | 微波消解 电感耦合等离子体-原子发射光谱法 海鸭蛋 金属元素 |
Determination of Metal Elements in Sea Duck Eggs by ICP-AES with Microwave Digestion |
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| LUO Hu , DENG Quan-Dao , XU Guang , LIANG De-Rong. Determination of Metal Elements in Sea Duck Eggs by ICP-AES with Microwave Digestion[J]. Chinese Journal of Spectroscopy Laboratory, 2012, 29(1): 314-316 |
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| Authors: | LUO Hu DENG Quan-Dao XU Guang LIANG De-Rong |
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| Affiliation: | a (Qinzhou Entry-Exit Inspection and Quarantine Bureau,Qinzhou,Guangxi 535000,P.R.China) a[China Certification & Inspection(Group) Guangxi Co.,Ltd.,Qinzhou,Guangxi 535000,P.R.China] |
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| Abstract: | A method was established to determine the metal elements in sea duck eggs by inductively coupled plasma atomic emission spectrometry(ICP-AES) with microwave digestion.The relative standard deviations(RSDs) of 15 elements were less than 2%(n = 12),and addition recoveries were in the range of 91.0%—105.4%.The method is simple and fast with high reliability,that can be applied to simultaneous determination of multi-element,that is suitable for rapid analysis and detection of sea duck eggs. |
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| Keywords: | Microware Digestion ICP-AES Sea Duck Eggs Metal Elements |
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