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Large volume sample application by a simplified “closed” on-column injector in capillary gas chromatography
Authors:R. W. Schmid  Ch. Wolf
Affiliation:(1) Laboratory of Psychoactive Drug Analysis, Psychiatric University Hospital of Vienna, Währinger Gürtel 18-20, A-1090 Vienna, Austria
Abstract:
Summary A new simplified version of a ldquoclosedrdquo on-column injector is introduced. Because of its design isobaric injection conditions do not have to be followed and a wide range of injection temperatures above the boiling point of the sample solvent can be chosen for on-column injections in capillary gas chromatography. Also, when following certain basic injection rules, injections of large sample volumes (ge20 mgrl or more) give accurate and reproducible results without further problems.Presented at the 17th International Symposium on Chromatography, September 25–30, 1988, Vienna, Austria.
Keywords:Gas chromatography  Large volume sample injection  Closed on-column injector
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