Triol protection with 6-benzoyl-3,4-dihydro-(2H)-pyran |
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| Authors: | Baker Caroline D L Fawcett John Insley Christopher D Messenger Derek S Newland Claire L Overend Helen L Patel Anup B Shah Mufakhrul Vara Bhavna Virdee Davinder Rawlings Bernard J |
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| Affiliation: | Department of Chemistry, University of Leicester, University Road, Leicester, UK. |
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| Abstract: | ![]()
6-Benzoyl-3,4-dihydro-(2H)-pyran will protect 1,2,3-triols such as glycerol as their corresponding spiro-[5-phenyl-3,6,8-trioxabicyclo[3.2.1]octane-4,2[prime or minute]-tetrahydropyran]s and 1,2,4-triols (less efficiently) as the corresponding trioxabicyclo[3.2.2]nonanes; the hexol mannitol is converted into the corresponding bis-protected product. |
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