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Comparison of microwave-assisted extraction of aloe-emodin in aloe with Soxhlet extraction and ultrasound-assisted extraction
Authors:WANG GuiHua  SU Ping  ZHANG Fan  HOU XiangYan  YANG Yi & GUO ZhenKu College of Science  Beijing University of Chemical Technology  Beijing   China Chinese Academy of Inspection    Quarantine  Beijing   China Beijing Rayleigh Analytical Instrument Co.  Beijing   China
Affiliation:WANG GuiHua1,SU Ping1,ZHANG Fan1,2,HOU XiangYan1,YANG Yi1 & GUO ZhenKu3 1College of Science,Beijing University of Chemical Technology,Beijing 100029,China 2Chinese Academy of Inspection and Quarantine,Beijing 100123,China 3Beijing Rayleigh Analytical Instrument Co.,Beijing 100016,China
Abstract:This paper reports the extraction of aloe-emodin from aloe by microwave-assisted extraction.The effects of various factors,including the solvent,the ratio (mL/g) of the solvent to the sample,microwave irradiation time and microwave power,were discussed in the experiments.The yield of aloe-emodin was determined by HPLC.The optimized conditions for microwave-assisted extraction of aloe-emodin were concluded as follows: the solvent is 80% ethanol (V/V) solution,microwave irradiation time is 3 min and microwave...
Keywords:microwave-assisted extraction  aloe  aloe-emodin  HPLC  fingerprint  transmission electronic microscopy  
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