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| 微波辐射下一步合成9-芳基-1,2,3,4,5,6,7,8,9,10-十氢-1,8-吖啶二酮 | |
| 引用本文： | 华国平,李团结,邹翔,屠树江,朱松磊,章晓镜,纪顺俊,张勇.微波辐射下一步合成9-芳基-1,2,3,4,5,6,7,8,9,10-十氢-1,8-吖啶二酮[J].有机化学,2005,25(10):1294-1297. |
| 作者姓名： | 华国平 李团结 邹翔 屠树江 朱松磊 章晓镜 纪顺俊 张勇 |
| 作者单位： | 1. 徐州建筑职业技术学院,徐州,221008;徐州师范大学化学系,江苏省药用植物生物技术重点实验室,徐州,221009 2. 徐州师范大学化学系,江苏省药用植物生物技术重点实验室,徐州,221009 3. 苏州大学化学化工学院,苏州,215006 |
| 基金项目： | 国家自然科学基金，江苏省自然科学基金，江苏省重点实验室基金，江苏省重点实验室基金 |
| 摘 要： | 以芳醛、1,3-环己二酮、醋酸铵为原料在无溶剂条件下经微波辐射合成了一系列9-芳基-1,2,3,4,5,6,7,8,9,10-十 氢-1,8-吖啶二酮. 该反应的反应时间短、产率高、环境友好、后处理方便. 产物的结构经红外光谱、核磁共振谱表征, 3d的结构经单晶X射线衍射进一步确证. |
| 关 键 词： | 芳醛 1 3-环己二酮 吖啶二酮 微波辐射 |
| 收稿时间： | 12 8 2004 12:00AM |
| 修稿时间： | 04 26 2005 12:00AM |
One-pot Synthesis of 9-Aryl-1,2,3,4,5,6,7,8,9,10-decahydro- 1,8-acridinedione under Microwave Irradiation |
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| HUA,Guo-Ping,LI,Tuan-Jie,ZOU,Xiang,TU,Shu-Jiang,ZHU,Song-Lei,ZHANG,Xiao-Jing,JI,Shui-Jun,ZHANG,Yong.One-pot Synthesis of 9-Aryl-1,2,3,4,5,6,7,8,9,10-decahydro- 1,8-acridinedione under Microwave Irradiation[J].Chinese Journal of Organic Chemistry,2005,25(10):1294-1297. | |
| Authors: | HUA Guo-Ping LI Tuan-Jie ZOU Xiang TU Shu-Jiang ZHU Song-Lei ZHANG Xiao-Jing JI Shui-Jun ZHANG Yong |
| Institution: | (Xuzhou Institute of Architectural Technology, Xuzhou 221008)(Key Laboratory of Biotechnology on Medical Plant of Jiangsu, Department of Chemistry, Xuzhou Normal University, Xuzhou 221009)(College of Chemistry and Chemical Engineering, Suzhou University, Suzhou 215006) |
| Abstract: | A series of 9-aryl-1,2,3,4,5,6,7,8,9,10-decahydro-1,8-acridinedione derivatives were synthesized via the reaction of aromatic aldehydes with 1,3-cyclohexanedione and ammonium acetate in solvent-free conditions under microwave irradiation by one-pot reaction. The reaction easily could be worked up with short reaction time, high yields and environmental friendliness. The structures of the products were con-firmed by IR and 1H NMR spectra. The structure of 3d was further determined by X-ray analysis. |
| Keywords: | aromatic aldehyde 1 3-cyclohexanedione microwave irradiation acridinedione |
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