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HPLC-ELSD同时检测肉产品中四环素类抗生素和己烯雌酚
引用本文:江勇,朱群英,倪永年,黄伟华.HPLC-ELSD同时检测肉产品中四环素类抗生素和己烯雌酚[J].南昌大学学报(理科版),2007,31(2):143-146.
作者姓名:江勇  朱群英  倪永年  黄伟华
作者单位:1. 南昌大学,食品科学教育部重点实验室,江西,南昌,330047;南昌市疾病预防控制中心,江西,南昌,330006
2. 南昌市疾病预防控制中心,江西,南昌,330006
3. 南昌大学,食品科学教育部重点实验室,江西,南昌,330047
基金项目:南昌市科学技术委员会重点攻关及产业化资助项目
摘    要:将高效液相色谱仪与蒸发光散射检测器联用,用C18柱实现了肉产品中3种四环素类抗生素和己烯雌酚的同时检测.探讨了不同流动相及ELSD参数对灵敏度的影响,对ELSD与紫外检测器进行了比较,并对实际样品进行了分析.

关 键 词:液相色谱  蒸发光散射检测器  四环素  己烯雌酚  同时检测  肉产品  四环素类抗生素  己烯雌酚  Diethylstilbestrol  Antibiotics  分析  样品  比较  紫外检测器  影响  灵敏度  参数  ELSD  流动相  检测器联用  蒸发光散射  液相色谱仪
文章编号:1006-0464(2007)02-0143-04
修稿时间:2006-08-03

Determination of Tetracyclines Antibiotics and Diethylstilbestrol by HPLC-ELSD
JIANG Yong,ZHU Qun-yin,NI Yong-nian,HUANG Wei-hua.Determination of Tetracyclines Antibiotics and Diethylstilbestrol by HPLC-ELSD[J].Journal of Nanchang University(Natural Science),2007,31(2):143-146.
Authors:JIANG Yong  ZHU Qun-yin  NI Yong-nian  HUANG Wei-hua
Institution:1. Key Laboratory of Food Science of Ministry of Education, Nanchang University, Nanchang 330047, China; 2. Nanchang Center for Disease Control and Prevention, Nanchang 330006, China
Abstract:A method,which determined simultaneously three kinds of tetracyclines antibiotics and diethylstilbestrol in meat product with C18 column by liquid chromatography coupled to evaporative light scattering detector, was described. Effects of different mobile phase and parameters of ELSD on the response were studied, and the ELSD was compared with UV detector. The real samples were analyzed.
Keywords:liquid chromatography  evaporative light scattering detector  tetracyclines antibiotics  diethylstilbestrol
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