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Preparation and characterization of silver/TiO2 composite hollow spheres
Authors:Song Caixia  Wang Debao  Gu Guohua  Lin Yusheng  Yang Jingyi  Chen Lei  Fu Xun  Hu Zhengshui
Affiliation:Department of Applied Chemistry, Qingdao University of Science and Technology, Qingdao, Shandong 266042, People's Republic of China.
Abstract:Silver-coated poly(methyl acrylic acid) (PSA) core-shell colloid particles were prepared by an in situ chemical reduction method. Crystalline silver/titania composite hollow spheres were obtained by coating the as-prepared PSA/silver particles with an amorphous titania layer and subsequently calcining in Ar atmosphere. SEM and TEM investigation indicated that the size of the as-prepared PSA/silver and PSA/silver/TiO(2) core-shell particles and silver/titania composite hollow particles was fairly uniform and the wall thickness of the hollow spheres was in the range of 40-80 nm. UV-vis absorption spectra were recorded to investigate their optical properties.
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