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Solid phase extraction and analysis of horse urine for aminocaproic acid |
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| Authors: | D. Phillips I. R. Tebbett S. Kalita |
| Affiliation: | (1) Dept. of Pharmacodynamics, University of Illinois at Chicago, P.O. Box 6998, 60680 Chicago, IL, USA;(2) Illinois Racing Board Laboratory, Elgin, IL, USA |
| Abstract: | Summary A rapid and efficient procedure is described for extraction and determination of aminocaproic acid in horse urine. Urine was extracted by passing through a bonded silica column (Bond-Elut). The adsorbed drug was washed free of endogenous materials before being eluted. The extract was then examined by thin-layer chromatography and HPLC. The purity of the extract was determined by gas chromatography-mass spectrometry. |
| Keywords: | Column liquid chromatography Thin-layer GC/MS Aminocaproic acid in horse urine Solid phase extraction |
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