New cyclization of N‐hydroxyiminoyl chlorides with N‐alkyl ethynesulfonamides: Synthesis of 4‐alkyl‐3‐aryl‐4,5‐dihydro‐1,5,2,4‐oxathiadiazepine‐5,5‐diones |
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Authors: | Yeon Soo Lee Kun Hoe Chung Yong Hae Kim |
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Abstract: | N‐Hydroxyiminoyl chlorides reacted with N‐alkyl ethynesulfonamides in the presence of triethylamine in CH2Cl2 to afford the 4‐alkyl‐3‐aryl‐4,5‐dihydro‐1,5,2,4‐oxathiadiazepine‐5,5‐diones (3) as the major products together with N‐alkyl‐3‐aryl‐5‐isoxazolesulfonamides (4). © 1999 John Wiley & Sons, Inc. Heteroatom Chem 10: 461–464, 1999 |
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