Abstract: | Syntheses and Properties of Bis(perfluoroalkyl)zinc Compounds The conditions for the syntheses of bis(perfluoroalkyl)zinc compounds Zn(Rf)2 · 2 D (Rf = C2F5, n‐C3F7, i‐C3F7, n‐C4F9, n‐C6F13, n‐C7F15, and n‐C8F17; D = CH3CN, tetrahydrofurane, dimethylsulfoxide) are described. Mass spectra, thermal decompositions, 19F‐ and 13C‐NMR spectra are discussed. |