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The crystal and molecular structure of 6,8,15,16b,16c,17-hexahydro-16b,16c-diphenyl-7H,16H-6a,7a,15a,16a-tetraazanaphtho[5,6]azulano[2,1,8-ij]naptho[f]azulene-7,16-dione
Authors:W. P. Bosman  J. M. M. Smits  R. de Gelder  J. N. H. Reek  R. J. M. Nolte
Affiliation:(1) Department of Organic Chemistry, Nijmegen SON Research Center, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands;(2) Department of Inorganic Chemistry, Nijmegen SON Research Center, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands;(3) RIM Laboratory of Solid State Chemistry, University of Nijmegen, Toernooiveld, 6525 ED Nijmegen, The Netherlands
Abstract:
The crystal and molecular structure of a clip containing molecule is described. The structure was solved by vector search methods and refined by least squares methods toRl=0.0768 [I>2sgr(I)]. Crystal data: C40H30N4O2·HCCl3, triclinic, space group
$$Pbar 1$$
,a=9.302(2),b=12.981(2),c=15.765(2)Å, agr=65.91(2)°, beta=76.40(2)°, gamma=80.15(1)°,V=1682.9(4)Å3, Z=2.
Keywords:Crystal structure  receptor  clip shaped molecule
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