Synthesis of TiO2/WO3 nanoparticles via sonochemical approach for the photocatalytic degradation of methylene blue under visible light illumination |
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Institution: | 1. Nanomaterials and Solar Energy Conversion Lab, Department of Chemistry, National Institute of Technology, Trichy 620 015, India;2. Department of Chemical Engineering, National Institute of Technology, Trichy 620 015, India;3. Institut Universitarid’Electroquímica, Departament de Química Física, Universitatd’Alacant, Apartat 99, E-03080 Alacant, Spain |
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Abstract: | Through an ultrasound assisted method, TiO2/WO3 nanoparticles were synthesized at room temperature. The XRD pattern of as-prepared TiO2/WO3 nanoparticles matches well with that of pure monoclinic WO3 and rutile TiO2 nanoparticles. TEM images show that the prepared TiO2/WO3 nanoparticles consist of mixed square and hexagonal shape particles about 8–12 nm in diameter. The photocatalytic activity of TiO2/WO3 nanoparticles was tested for the degradation of a wastewater containing methylene blue (MB) under visible light illumination. The TiO2/WO3 nanoparticles exhibits a higher degradation rate constant (6.72 × 10?4 s?1) than bare TiO2 nanoparticles (1.72 × 10?4 s?1) under similar experimental conditions. |
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Keywords: | Sonochemical synthesis TEM Photocatalysis Methylene blue |
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