Preparation and Characterization of NiO Nanoparticles via Solid-State Thermal Decomposition of Ni(II) Complex |
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Authors: | Aliakbar Dehno Khalaji |
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Institution: | 1. Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran
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Abstract: | Nickel(II) complex, Ni(Brsalph)(NO3) was synthesized and characterized by elemental analyses and Fourier-transformed infrared (FT-IR) spectroscopy. Heating of Ni(Brsalph)(NO3) at 550 °C for 3.5 h have resulted NiO nanoparticles. Fourier-transformed infrared spectrum confirmed the composition of products. The crystalline structures and morphology of NiO nanoparticles were studied by X-ray powder diffraction, scanning electron microscopy and transmission electron microscopy. |
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