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Synthesis and Characterization of CdS Nanoparticles via Cyclic Microwave from Cadmium Oxalate
Authors:Masoud Salavati-Niasari  Sanaz Khoshroozi  Mohammad Sabet
Institution:1. Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, P.O. Box 87317-51167, Kashan, Islamic Republic of Iran
2. Institute of Nano Science and Nano Technology, University of Kashan, P.O. Box 87317-51167, Kashan, Islamic Republic of Iran
3. Department of Chemistry, Faculty of Science, Sanandaj Branch, Islamic Azad University, Sanandaj, Iran
Abstract:The present study reports synthesis and characterization of CdS nanoparticles prepared by cyclic microwave route with the use of Cd(C2O4)·3H2O] powder as a precursor. The products, with an average size ~15 nm, were characterized by X-ray diffraction, scanning electron microscopy, energy dispersive X-ray microanalysis, thermogravimetric analysis, transmission electron microscopy and Fourier transform infrared spectroscopy. Optical property of obtained product was investigated by photoluminescence spectroscopy. The prepared nanostructures displayed a very strong luminescence at 528 nm (2.34 eV) at room temperature.
Keywords:
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