Investigation of failure mechanisms in polymer composites by simultaneous measurement of ultra-small-angle scattering and acoustic emission during the deformation. I. Method
1. Department of Experimental Physics , University of Ulm , D-89069, Ulm, Germany;2. Department of Experimental Physics , University of Ulm , D-89069, Ulm, Germany;3. HASYLAB at DESY , D-22607, Hamburg, Germany
Abstract:
Failure mechanisms in polymer composites were investigated with the method of ultra-small-angle X-ray scattering using synchrotron radiation and acoustic emission analysis simultaneously. The composites were prepared from polystyrene filled with glass beads with different coatings. The two-dimensional scattering patterns were analyzed by means of a cylinder model, while the curves of the acoustic emission signals per stress or amplitude interval were calculated and fitted by a Weibull distribution function.