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Investigation of failure mechanisms in polymer composites by simultaneous measurement of ultra-small-angle scattering and acoustic emission during the deformation. I. Method
Authors:A Karl  S Cunis  R Gehrke  G v Krosigk  U Lode  I Luzinov
Institution:1. Department of Experimental Physics , University of Ulm , D-89069, Ulm, Germany;2. Department of Experimental Physics , University of Ulm , D-89069, Ulm, Germany;3. HASYLAB at DESY , D-22607, Hamburg, Germany
Abstract:Failure mechanisms in polymer composites were investigated with the method of ultra-small-angle X-ray scattering using synchrotron radiation and acoustic emission analysis simultaneously. The composites were prepared from polystyrene filled with glass beads with different coatings. The two-dimensional scattering patterns were analyzed by means of a cylinder model, while the curves of the acoustic emission signals per stress or amplitude interval were calculated and fitted by a Weibull distribution function.
Keywords:Acoustic emission monitoring  Failure mechanisms  Polymer composites  Small-angle X-ray scattering  
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