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白芷的提取工艺
引用本文:索建兰,袁佳妹.白芷的提取工艺[J].光谱实验室,2012,29(3):1620-1623.
作者姓名:索建兰  袁佳妹
作者单位:宝鸡文理学院化学化工系 陕西省宝鸡市高新大道1号 721013
基金项目:陕西省植物化学重点实验室重点项目,陕西省教育厅项目
摘    要:探讨多因素实验条件对白芷的提取工艺参数的影响,以欧前胡素和异欧前胡素的含量为指标,以乙醇浓度、乙醇用量、提取时间、提取次数为因素进行单因素试验。结果表明,白芷的最佳提取工艺参数为:以8倍量80%乙醇提取3次,每次lh。

关 键 词:白芷  欧前胡素  异欧前胡素  高效液相色谱  乙醇回流提取  浸泡提取

Extraction Process of Radix Angelicae Dahuricae
SUO Jian-Lan , YUAN Jia-Mei.Extraction Process of Radix Angelicae Dahuricae[J].Chinese Journal of Spectroscopy Laboratory,2012,29(3):1620-1623.
Authors:SUO Jian-Lan  YUAN Jia-Mei
Institution:SUO Jian-Lan YUAN Jia-Mei(Department of Chemistry and Chemical Engineering,Baoji University of Arts and Sciences,Baoji,Shaanxi 721013,P.R.China)
Abstract:The parameters of extraction process Radix Angelicae Dahuricae were optimized by single factor test,with the contents of imperatorin and isomperatorin as index,and the factors of orthogonal design were carried out,the factors including the concentration of ethanol,the dosage of ethanol,the extraction time and extraction times.The results indicated that the optimal extraction process was obtained as follows: the ethanol concentration of 80% for 8 times dosage and the extraction times of 3 for each time of 1h.
Keywords:Radix Angelicae Dahuricae  Imperatorin  Isomper atorin  High Performance Liquid Chromatography  Ethanol Reflux Extraction  Immersion Extraction
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