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SrSnO3纳米粒子的制备及其光催化性能
引用本文:王红军,薛洪滨,朱光辉,曾翠平,关梦杰,杨术明.SrSnO3纳米粒子的制备及其光催化性能[J].光谱实验室,2012,29(4):1952-1955.
作者姓名:王红军  薛洪滨  朱光辉  曾翠平  关梦杰  杨术明
作者单位:信阳师范学院化学化工学院应用化学研究所 河南省信阳市长安路237号 464000
基金项目:国家自然科学基金项目,信阳师范学院青年基金资助项目
摘    要:以硝酸锶Sr(NO32]和结晶四氯化锡(SnCI4·5H2O)为原料,有机碱四甲基氢氧化铵N(CH34OH]为矿化剂,采用共沉淀法制备SrSnO3纳米粒子。用XRD和IR对样品的物相和结构进行表征,并研究了对亚甲基蓝废水的光催化降解性能。结果表明:用该法在500℃煅烧1h时制备的纯立方相SrSnO3纳米晶粒在可见光照下具有良好的光催化性能。催化剂浓度为60mg/L,反应时间为100min时,降解率可达94%。

关 键 词:共沉淀法  SrSnO3纳米粒子  有机碱四甲基氢氧化铵  光催化隆解

Preparation and Photocatalytic Properties of SrSnO3 Nanoparticles
WANG Hong-Jun , XUE Hong-Bin , ZHU Guang-Hui , ZENG Cui-Ping , GUAN Meng-Jie , YANG Shu-Ming.Preparation and Photocatalytic Properties of SrSnO3 Nanoparticles[J].Chinese Journal of Spectroscopy Laboratory,2012,29(4):1952-1955.
Authors:WANG Hong-Jun  XUE Hong-Bin  ZHU Guang-Hui  ZENG Cui-Ping  GUAN Meng-Jie  YANG Shu-Ming
Institution:Wang Hong-Jun Xue Hong-Bin Zhu Guang-Hui Zeng Cui-Ping GuAN Meng-Jie Yang Shu-Ming (College oj Chemistry and Chemical Engineering,Institute of Applied Chemistry Xinyang Normal University, Xinyang,Henan 464000,P.R.China)
Abstract:Perovskite SrSnO3 nanoparticles were synthesised by co-precipitation method using Sr(NO32 and SnCl4 · 5H2O as materials and the organic base tetramethyl ammonium hydroxide N(CH34OH]as mineralizer.The phases and microstructure were characterized by XRD and IR.Its photocatalytic activity to the methylene blue was investigated.When the pure cubic phase SrSn03 nanoparticles synthesized at 500℃for 1h was irradiated by the visible light,the photo-degradation of methylene blue could reach to 9A%as the concentraion of photocatalyst was 60mg/L and the reaction time was 100min.
Keywords:Co-precipitation Method  SrSnO3 Nanoparticles  Organic Base Tetramethyl Ammonium Hydroxide  Photocatalytic Degradation
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