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分光光度法研究插层膨润土负载掺氮TiO2光催化剂对亚甲基蓝的光降解
引用本文:陈慧娟,张敬华,杨莹琴. 分光光度法研究插层膨润土负载掺氮TiO2光催化剂对亚甲基蓝的光降解[J]. 光谱实验室, 2012, 29(4): 1998-2001
作者姓名:陈慧娟  张敬华  杨莹琴
作者单位:1. 信阳师范学院化学化工学院 河南省信阳市长安路237号 464000
2. 黄淮学院化学化工系 河南省驻马店市 463000
基金项目:河南省科技厅科技攻关项目,河南省教育厅资助项目
摘    要:
采用溶胶-凝胶法制备了具有高活性的可见光响应插层膨润土负载掺氮TiO2光催化剂(以下简称光催化剂)。利用IR对光催化剂的微观结构进行表征,并以亚甲基蓝为目标降解物,讨论了光催化剂在可见光下的催化活性。结果表明:氮掺杂TiO2成功负载于插层膨润土片层表面。在尿素掺杂量为0.35g和催化剂用量为40mg条件下,光催化剂对25mL初始浓度为5mg/L的亚甲基蓝溶液的降解率可达99%。

关 键 词:插层膨润土  掺氮TiO2  光催化剂  制备  光隆解

Photodegradation of Intercalated Bentonite Loaded Nitrogen-Doped TiO2 Photocatalysts on Methylene Blue by Spectrophotometry
CHEN Hui-Juan , ZHANG Jing-Hua , YANG Ying-Qin. Photodegradation of Intercalated Bentonite Loaded Nitrogen-Doped TiO2 Photocatalysts on Methylene Blue by Spectrophotometry[J]. Chinese Journal of Spectroscopy Laboratory, 2012, 29(4): 1998-2001
Authors:CHEN Hui-Juan    ZHANG Jing-Hua    YANG Ying-Qin
Affiliation:Chen Hui-Juan Zhang Jing-Huaa Yang Ying-Qin (College of Chemistry and Chemical Engineering,Xinyang Normal University,Xinyang,Henan 464000,P.R.China) a(College of Chemistry and Chemical Engineering,Huanghuai University,Zhumadian,Henan 463000,P.R.China)
Abstract:
Highly efficient visible-light-induced intercalated bentonite loaded nitrogen-doped TiO2 photocatalystsCphotocatalysts for short)were produced by sol-gel method.The micro-structure of the photocatalysts was characterized by IR,and photocatalytic activity of photocatalysts under visible-light irradiation was discussed with the methylene blue as target degradation products.The results demonstrated that the nitrogen-doped TiO2 was successfully loaded on the surface of the intercalated bentonite.In conditions of the CO(NH22 mass of 0.35g and the photocatalysts mass of 40mg,the degradation rate reached 99%for photocatalysts on the methylene blue initial concentration of 5mL/L for 25mL.
Keywords:Intercalated Bentonite  Nitrogen-Doped TiO2  Photocatalyst  Production  Photodegradation
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