Combination of (13)C-(13)C COSY and DARR (COCODARR) in solid-state NMR |
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| Authors: | Fukuchi Masashi Takegoshi K |
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| Institution: | Division of Chemistry, Graduate School of Science, Kyoto University, Kyoto 606-8502, Japan. muku@kuchem.kyoto-u.ac.jp |
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| Abstract: | In this work, we describe a new 2D (13)C-(13)C correlation experiment in solids, in which (13)C-(13)C J-correlation (COSY) and dipolar correlation (DARR) are recorded at the same time. The sequence is similar to COCONOSY in the liquid-state NMR, in which (1)H-(1)H COSY and NOESY spectra are obtained in a single experiment. The combined COSY and DARR experiment facilitates assignment of (13)C signals in solids. |
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