Synthesis and Characterization of Novel Arylaldehyde (Arylketone)‐(4‐Substituted phenyl‐5‐Substituted phenoxy‐Methyl‐4H‐1,2,4‐Triazole‐3‐yl)‐Thiol Acetyl Hydrazones |
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| Authors: | Heng‐Wen Zhang Yan‐Ping Li Chen‐Jiang Liu Hai‐Long Li Wen‐Li Sun |
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| Institution: | Key Laboratory of Oil and Gas Fine Chemicals of Ministry of Education, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi Xinjiang 830046, P. R. China |
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| Abstract: | Fourteen novel arylaldehyde (arylketone)‐(4‐substituted phenyl‐5‐substituted phenoxy‐methyl‐4H‐1,2,4‐triazole‐3‐yl)‐thiol acetyl hydrazone derivatives ( 5a‐5g, 6a‐6g ) were synthesized by 4‐substituted phenyl‐5‐substituted phenoxy‐methyl‐1,2,4‐triazole‐3‐thione as starting material according to substructure link principle, followed by thioetherification, hydrazide hydrazone reaction. The structures of these compounds were confirmed by IR, 1H NMR and elemental analysis. Crystal structure of compounds 1b and 6d were determined by the X‐ray diffraction. |
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| Keywords: | Hydrazone derivatives 1 2 4‐Triazole Synthesis Crystal structureas |
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