| 加速溶剂萃取法提取烟叶挥发性成分条件的优化 |
| |
| 引用本文： | 黄兰芳,胡伟,谢建伟,王玉林.加速溶剂萃取法提取烟叶挥发性成分条件的优化[J].光谱实验室,2010,27(4):1406-1410. |
| |
| 作者姓名： | 黄兰芳 胡伟 谢建伟 王玉林 |
| |
| 作者单位： | 衢州学院化学与制药工程系,浙江省衢州市九华北大道78号,324000 |
| |
| 摘 要： | 以色谱指纹图谱信息量为指标,用正己烷为萃取剂,采用均匀设计法优化了萃取时间、萃取温度和泵入萃取池溶剂量占池体积百分数3个因素对加速溶剂萃取法萃取烟叶挥发性成分的影响,由此提出了一快速测定烟叶挥发性成分的方法。所得萃取液用气相色谱-质谱联用(GC-MS)检测后,用NIST质谱数据库检索进行定性分析,共鉴定出44种化学组分,占挥发油总量的88.87%,所得结果能为烟叶化学成分的研究提供有利的科学依据。
|
| 关 键 词： | 气相色谱-质谱法 烟叶 挥发性成分 加速溶剂萃取 均匀设计 |
Optimization of Extraction Conditions for the Extraction of Volatile Components in Cut Tobacco with Accelerated Solvent Extraction |
| |
| HUANG Lan-Fang,Hu Wei,XIE Jian-Wei,WANG Yu-Lin.Optimization of Extraction Conditions for the Extraction of Volatile Components in Cut Tobacco with Accelerated Solvent Extraction[J].Chinese Journal of Spectroscopy Laboratory,2010,27(4):1406-1410. |
| |
| Authors: | HUANG Lan-Fang Hu Wei XIE Jian-Wei WANG Yu-Lin |
| |
| Institution: | (Department of Chemistry and Pharmaceutical Engineering,Quzhou College,Quzhou,Zhejiang 324000,P.R.China) |
| |
| Abstract: | The volatile components in cut tobacco were extracted with accelerated solvent extraction （ASE） and n-hexane.The extraction conditions,namely time,temperature and the percent of solvent,were investigated by information content of chromatograph fingerprint and uniform design method.The volatile components in cut tobacco were detected by GC-MS,and identified by similarity search in NIST library.A total of 44 components were identified,accounting for 88.87% of the total content.The obtained results can provide useful information for the study of chemical components in cut tobacco. |
| |
| Keywords: | GC-MS Cut Tobacco Volatile Components Accelerated Solvent Extraction Uniform Design |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
