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千里光中几种黄酮和酚酸类成分的分离与鉴定
引用本文:何忠梅,宗颖,孙佳明,肖凤艳. 千里光中几种黄酮和酚酸类成分的分离与鉴定[J]. 应用化学, 2010, 27(12): 1486-1488. DOI: 10.3724/SP.J.1095.2010.00061
作者姓名:何忠梅  宗颖  孙佳明  肖凤艳
作者单位:(1.吉林农业大学中药材学院 长春130116;2.长春中医药大学中医药与生物工程研究开发中心 长春;3.吉林农业科技学院 吉林)
基金项目:吉林省教育厅"十一五"科研规划,吉林农业大学科研启动基金
摘    要:
对千里光(Senecio scandens Buch.-Ham.)全草的乙酸乙酯提取部位进一步分离,得到4个黄酮类化合物和2个酚酸类化合物,经理化性质和NMR及MS谱学数据鉴定分别为槲皮素3-O-β-D-葡萄糖苷(Ⅰ)、金丝桃苷(Ⅱ)、槲皮素(Ⅴ)、异鼠李素(Ⅵ)、绿原酸(Ⅲ)和咖啡酸(Ⅳ)。 其中化合物Ⅰ~Ⅵ均为首次从千里光属植物中分离鉴定。

关 键 词:千里光  黄酮  酚酸  分离  鉴定  
收稿时间:2010-01-25
修稿时间:2010-03-14

Isolation and Identification of Several Flavonoids and Phenolic Acids from Senecio scandens Buch.-Ham.
HE Zhong-Mei,ZONG Ying,SUN Jia-Ming,XIAO Feng-Yan. Isolation and Identification of Several Flavonoids and Phenolic Acids from Senecio scandens Buch.-Ham.[J]. Chinese Journal of Applied Chemistry, 2010, 27(12): 1486-1488. DOI: 10.3724/SP.J.1095.2010.00061
Authors:HE Zhong-Mei  ZONG Ying  SUN Jia-Ming  XIAO Feng-Yan
Affiliation:(1.College of Chinese Medicine Materials,Jilin Agricultural University,Changchun 130116;;2.Development Center of Traditional Chinese Medicine and Bioengineering,;Changchun University of Traditional Chinese Medicine,Changchun;3.Jilin Agricultural Science and Technology College,Jilin)
Abstract:
Further separation of the ethyl acetate extractive of Senecio scandens Buch.-Ham., four flavonoids and two phenolic acids were isolated by chromatography and identified by physico-chemical properties, NMR and MS, as isoquercitrin(Ⅰ), hyperin(Ⅱ), chlorogenic acid(Ⅲ), caffeic acid(Ⅳ), quercetin(Ⅴ) and isorhamnetin(Ⅵ). Compound Ⅰ was isolated from plant of Senecio genus for the first time, and compounds Ⅱ~Ⅵ were isolated from the plant for the first time.
Keywords:Senecio scandens Buch.-Ham.  flavonoids  phenolic acids  isolation  identification
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