| 通过加成反应制备纳米材料的新方法 |
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| 引用本文： | 王博,张秀娟,张晓宏. 通过加成反应制备纳米材料的新方法[J]. 影像科学与光化学, 2009, 27(4): 280-286. DOI: 10.7517/j.issn.1674-0475.2009.04.280 |
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| 作者姓名： | 王博 张秀娟 张晓宏 |
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| 作者单位： | 中国科学院理化技术研究所,北京100190;中国科学院研究生院,北京100049;中国科学院理化技术研究所,北京,100190 |
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| 摘 要： | 通过加成反应,结合再沉淀法,制备得到Ni(DMG)2的单晶纳米结构,并且通过调节反应物浓度可实现不同形貌的可控生长,在浓度低的条件下,可得到六方纳米管材,而随着浓度的升高,逐渐变为实心的六方纳米棒,这种制备方法提供了一种潜在的新方法——即通过加成反应来制备纳米材料。
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| 关 键 词： | 加成反应 纳米材料 丁二酮肟镍螯合物 |
| 收稿时间： | 2009-01-20 |
A New Method to Prepare Single-crystal Nanomaterial via"Addition Reaction" |
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| WANG Bo,ZHANG Xiu-juan,ZHANG Xiao-hong. A New Method to Prepare Single-crystal Nanomaterial via"Addition Reaction"[J]. Imaging Science and Photochemistry, 2009, 27(4): 280-286. DOI: 10.7517/j.issn.1674-0475.2009.04.280 |
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| Authors: | WANG Bo ZHANG Xiu-juan ZHANG Xiao-hong |
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| Affiliation: | 1. Technical Institute of Physics and Chemistry, Chinese Academy of Sciences, Beijing 100190, P. R. China;2. Graduate University of the Chinese Academy of Sciences, Beijing 100049, P. R. China |
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| Abstract: | A reliable and facile new method to prepare Ni(DMG)2 single-crystal nanomaterials was demonstrated.Single-crystal 1D nano rods and tubes with controllable size and morphology were synthesized by using classic addition reaction following with precipitation process.It provided a new method for the preparation of nanomaterials.The concentration of the reactants used as a key effective tuning parameter had been found in the work for the shape evolution. |
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| Keywords: | addition reaction nano-material Nickel dimethylglyoxime chelate |
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