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Synthesis of dimethylditritiogermane Me |
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| Authors: | D. L. Myalochkin T. A. Kochina D. V. Vrazhnova V. V. Avrorin E. N. Sinotova |
| Affiliation: | (1) Grebenshchikov Institute of Silicate Chemistry, Russian Academy of Sciences, ul. Odoevskogo 24, korp. 2, St. Petersburg, 199155, Russia;(2) St. Petersburg State University, St. Petersburg, Russia |
| Abstract: | A microsynthetic procedure for preparing tritium-labeled alkyl-substituted germanes is developed. The resulting dimethylditritiogermane can be used as a source of dimethylgermylium ions. The synthesis was performed by the reduction of dibromodimethylgermane with lithium tritide in presence of AlBr3. |
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