| Synthesis of di-μ-OXO-tetra-（α-pentyloxy） tin（Ⅳ） phthalocyanine |
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| 作者姓名： | Yi Ru Peng Yu Hong Cao Pei Feng Chen Xiao Xia Huang |
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| 作者单位： | College of Chemistry & Material Science, Fujian Normal University, Fuzhou 350007, China |
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| 基金项目： | This study was supported by the National Natural Science Foundation of China (No. 20604007), Natural Science Foundation of Fujian (No. C0510007), Key Foundation for Ministry of Education, China (No. 206071), Key Foundation for Technology Department (2007I0013), Key Foundation for Education Office of Fujian (No. JA05195). |
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| 摘 要： | Axially substituted tin phthalocyanines, namely dichloride-tetra-（α-pentyloxy） tin （Ⅳ） phthalocyanine 2, dihydroxy-tetra-（α-pentyloxy） tin （Ⅳ） phthalocyanine 3 and its dimmer di-μ-oxo-tetra-（α-pentyloxy） tin（Ⅳ） phthalocyanine 4 were synthesized. The catalytic effect of H2O-free CaCl2 in quinoline was used for condensation of dihydroxy tin phthalocyanine 3 to the cofacially array dimmer 4. Their structures were characterized by UV-vis, IR, elemental analysis, MS, as well as ^1HNMR spectroscopy.
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| 关 键 词： | 轴向取代 酞菁染料 调光器 合成方法 |
| 收稿时间： | 24 September 2007 |
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