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A facile synthesis of 1-cycloalkenyl isothiocyanates with silicon tetraisothiocyanate |
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| Authors: | Ichiro Mori Koichiro Oshima Hitosi Nozaki |
| Affiliation: | Department of Industrial Chemistry, Faculty of Engineering, Kyoto University, Yoshida, Kyoto 606, Japan |
| Abstract: | The reaction of cycloalkanones with silicon tetraisothiocyanate in the presence of (Me3SiO)2SO2?nBu3SnF or Zn(NCS)2 provides 1-cycloalkenyl isothiocyanates in good yields under mild conditions. |
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