New synthesis of 1-triacontanol |
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Authors: | UT Bhalerao SJagadishwar Rao BD Tilak |
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Institution: | Regional Research Laboratory, Hyderabad-500 007, India;Indian Institute of Education, 128/2, Karve Road, Kothrud, Pune, India. |
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Abstract: | Succinic anhydride and behenic acid have been used to attach C4 and C22 carbon chains on to 2 and 5 positions of thiophene through two alternate acylation sequences. Raney nickel desulphurization to the 2,5-disubstituted thiophene yielded triacontanoic acid esters which on LAH reduction gave 1-triacontanol. |
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