| O-烷基,O-芳基硫代磷酰取代硫脲和O-烷基硫代磷酰-双-取代硫脲的研究(Ⅱ) |
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| 引用本文： | 胡式贤,姜恒.O-烷基,O-芳基硫代磷酰取代硫脲和O-烷基硫代磷酰-双-取代硫脲的研究(Ⅱ)[J].高等学校化学学报,1994,15(11):1634-1638. |
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| 作者姓名： | 胡式贤 姜恒 |
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| 作者单位： | 辽宁师范大学化学系, 大连, 116022 |
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| 基金项目： | 辽宁省教育委员会重点学科基金 |
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| 摘 要： | 用硫氰酸钾与硫代磷酰氯制备了硫代磷酰异硫氰基酯和二异硫氰基酯,并以其与不同胺反应,合成了硫代磷酰取代硫脲和硫代磷酰-双-取代硫脲两系列20个新的有机磷化合物,经1HNMR、IR及元素分析确定了它们的化学结构,测定了它们的生物活性。结果表明只有O-异丙基,O-(4-甲基-2-硝基苯基)-N''-萘基硫代磷酰硫脲(PD-1)具有较好的杀菌活性。
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| 关 键 词： | O－烷基 O－芳基硫代磷酰取代硫脲 O－烷基硫代磷酰双取代硫脲 杀菌活性 |
| 收稿时间： | 1993-11-08 |
Studies on O-Alkyl,O-arylphosphoro(thioureido)thioates and O-Alkylphosphoro-bis-(thioureido)thioates |
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| HU Shi-Zian,JIANG Heng,WANG Ping.Studies on O-Alkyl,O-arylphosphoro(thioureido)thioates and O-Alkylphosphoro-bis-(thioureido)thioates[J].Chemical Research In Chinese Universities,1994,15(11):1634-1638. |
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| Authors: | HU Shi-Zian JIANG Heng WANG Ping |
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| Institution: | Department of Chemistry, Liaoning Normal University, Dalian, 116022 |
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| Abstract: | From thiopliosphorylchloride and potassium thiocyanate, series of phosphoro(isothiocyanatido)thioates and phosphoro-bis(isothiocyanatido)thioates were prepared, andthen through the reactions of these componds with amines two series of new oganic phosphorus compounds(RO)(ArO)P(S)NHC(S)NR1R2 and(RO)P(S)NHC(S)NR1R2]2 were prepared.The structures of these compounds have been confirmed by IR, NMR, and elementary analysis.The results from the preliminary bioassay showed that compound PD-1 has fairlygood bactericidal activity. |
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| Keywords: | O-alkyl O-arylphosphoro(thioureido)thioates O-alkylphosphoro-bis-(thioureido)thioates Bactericidal activity |
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