|
|||||
|
|
| SYNTHESIS AND CHARACTERIZATION OF N-（1-NAPHTHYL） SUCCINIMIDE | |
| 引用本文： | LI Hexian YANG Hailong LIU Kun WANG Ying YUAN Jialong WANG Guochang. SYNTHESIS AND CHARACTERIZATION OF N-（1-NAPHTHYL） SUCCINIMIDE[J]. 反应性高分子(英文版), 2007, 16(1): 1-6 |
| 作者姓名： | LI Hexian YANG Hailong LIU Kun WANG Ying YUAN Jialong WANG Guochang |
| 作者单位： | LI Hexian（Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China） ;YANG Hailong（Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China） ;LIU Kun（Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China） ;WANG Ying （Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China） ;YUAN Jialong（Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China） ;WANG Guochang（Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China） ; |
| 基金项目： | 国家自然科学基金 , 天津市自然科学基金 |
| 摘 要： | In this paper a modified two-step procedure for synthesis of N-（1-naphthyl） suecinimide （NaS） was developed, and the molecular structure of NaS was properly characterized by XRD, FT-IR, 1H NMR, DSC, etc. The results show that the melting point of our product is 159 ℃-160.5 ℃, and the characteristic infrared absorption band of carbonyl group splits into two peaks （1705cm^-3/1779cm^-3）, which are found to be quite different from the documented data （rap 147℃ -149℃; IR C=0-1700cm^-3）. Besides, photophysical spectroscopy was found to be powerful to study the molecular structure and crystal morphology of NaS compound. |
| 关 键 词： | N-(1-萘基) 琥珀酰亚胺 微居里 高分子物理 |
SYNTHESIS AND CHARACTERIZATION OF N-(1-NAPHTHYL) SUCCINIMIDE |
|
| LI Hexian,YANG Hailong,LIU Kun,WANG Ying,YUAN Jialong,WANG Guochang. SYNTHESIS AND CHARACTERIZATION OF N-(1-NAPHTHYL) SUCCINIMIDE[J]. Chinese Journal of Reactive Polymers, 2007, 16(1): 1-6 | |
| Authors: | LI Hexian YANG Hailong LIU Kun WANG Ying YUAN Jialong WANG Guochang |
| Affiliation: | Institute of Polymer Chemistry, Nankai University, Tianjin 300071, China |
| Abstract: | In this paper a modified two-step procedure for synthesis of N-(1-naphthyl) succinimide (NaS) was developed, and the molecular structure of NaS was properly characterized by XRD, FT-IR,1H NMR, DSC, etc. The results show that the melting point of our product is 159 ℃～160.5 ℃, and the characteristic infrared absorption band of carbonyl group splits into two peaks (1705cm-1/1779cm-1),which are found to be quite different from the documented data (mp 147 ℃～149 ℃; IR C=O,～1700cm-1 ). Besides, photophysical spectroscopy was found to be powerful to study the molecular structure and crystal morphology of NaS compound. |
| Keywords: | N-(1-naphthyl) succinimide Microcrystals Infrared spectrum Fluorescence spectra. |
| 本文献已被 维普 万方数据 等数据库收录！ | |