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平面双核酰亚胺酞菁铁的激光解吸电离飞行时间质谱分析
引用本文:季怡萍,张红明. 平面双核酰亚胺酞菁铁的激光解吸电离飞行时间质谱分析[J]. 分析测试技术与仪器, 2008, 14(3): 144-146
作者姓名:季怡萍  张红明
作者单位:中国科学院,长春应用化学研究所,吉林,长春,130022;中国科学院,长春应用化学研究所,吉林,长春,130022
摘    要:
应用激光解吸电离飞行时间质谱法(LDI—TOF—MS)对平面双核酰亚胺酞菁铁相对分子量进行了测定.探讨了3种不同基质对其分析结果的影响,结果发现基质并不能完全解离样品,而不加任何基质的激光质谱得到了理想的结果.

关 键 词:平面双核酰亚胺酞菁铁  激光解析电离飞行时间质谱
收稿时间:2008-06-26
修稿时间:2008-08-08

Characterization of Planar Binuclear Iron Phthalocyanine Using Laser Desorption Ionization Time of Flight Mass Spectrometry
JI Yi-ping and ZHANG Hong-ming. Characterization of Planar Binuclear Iron Phthalocyanine Using Laser Desorption Ionization Time of Flight Mass Spectrometry[J]. Analysis and Testing Technology and Instruments, 2008, 14(3): 144-146
Authors:JI Yi-ping and ZHANG Hong-ming
Affiliation:JI Yi-ping, ZHANG Hong-ming (Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022, China)
Abstract:
Relative molecular weight of planar binuclear iron phthalocyanine was successfully determined by laser desorption ionization time of flight mass spectrometry(LDI-TOF-MS) technique.The effect of three kinds of matrix on the analytical result was investigated,however,the matrix hasn't improved the quality of spectra.The LDI-TOF-MS technique without addition of any matrix was found to provide better results for this kind of compound.
Keywords:planar binuclear iron phthalocyanine  laser desorption ionization time-of-flight mass spectrometry(LDI-TOF-MS)
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