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紫外分光光度法测定非诺贝特片含量的不确定度评定
引用本文:李宇,刘洪海. 紫外分光光度法测定非诺贝特片含量的不确定度评定[J]. 光谱实验室, 2010, 27(1): 283-286
作者姓名:李宇  刘洪海
作者单位:德州学院中专部山东省德州市大学西路566号,253023;德州市药品检验所,山东省德州市天衙中路433号,253015
摘    要:分析了非诺贝特片含量测定过程中样品的称样量、含量的重复性测量、样品的稀释体积和紫外分光光度法测量吸光度等因素对含量测定不确定度的影响。量化了各分量的相对标准不确定度,进而得出合成标准不确定度和扩展不确定度。建立的不确定度评定方法适用于分光光度法测定非诺贝特片含量的不确定度分析。

关 键 词:紫外分光光度法  不确定度  非诺贝特片

Evaluation of Uncertainty Measurement in the Content Determination of Fenofibrate Tablets by Ultraviolet Spectrophotometry
LI YU,LIU Hong-Hai. Evaluation of Uncertainty Measurement in the Content Determination of Fenofibrate Tablets by Ultraviolet Spectrophotometry[J]. Chinese Journal of Spectroscopy Laboratory, 2010, 27(1): 283-286
Authors:LI YU  LIU Hong-Hai
Affiliation:Dezhou University Technical Secondary School;Dezhou;Shandong 253023;P.R.China;Dezhou Institute for Drug Control;Shandong 253015;P.R.China
Abstract:The uncertainty in the determination of fenofibrate tablets was from weight of sample,analyzed,including repeatability of results of measurements,the dilated sample,the measurement by ultraviolet spectrophotometry.The combined standard uncertainty was obtained by combining each standard uncertainty,then the expanded uncertainty can be obtained.The uncertainty assessment method established can be used for uncertainty analysis of determination of fenofibrate tablets with spectrophotometry.
Keywords:Ultraviolet Spectrophotometry  Uncertainty  Fenofibrate Tablets  
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