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Rapid solidification processing in molten salts chemistry: X-ray analysis of deeply undercooled cryolite-alumina melts
Authors:Michal Korenko  Marián Kucharík  Dušan Janičkovič
Affiliation:(1) Institute of Inorganic Chemistry, Slovak Academy of Sciences, Dúbravská cesta 9, SK-845 36 Bratislava, Slovak Republic;(2) Institute of Physics, Slovak Academy of Sciences, Dúbravská cesta 9, SK-845 36 Bratislava, Slovak Republic
Abstract:Rapid solidification processing (cooling rate from the interval 105–106 K s−1) was used to prepare deeply undercooled cryolite-alumina melts. Such prepared samples were analyzed by the XRD method. Besides cryolite, XRD patterns belonging to ι-Al2O3 were recorded. The influence of annealing on the XRD patterns of deeply undercooled melts was also investigated.
Keywords:rapid solidification processing  cryolite-alumina melt  XRD  deeply undercooled melts
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