| ZnO纳米线的电化学制备研究 |
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| 引用本文： | 孟阿兰,蔺玉胜,王光信.ZnO纳米线的电化学制备研究[J].无机化学学报,2005,21(4):583-587. |
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| 作者姓名： | 孟阿兰 蔺玉胜 王光信 |
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| 作者单位： | 青岛科技大学化学与分子工程学院,青岛,266042 |
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| 基金项目： | 国家自然科学基金资助项目(No.50132040)。 |
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| 摘 要： | High-quality ZnO nanowires have been synthesized at relatively low temperature via one-step electrochemical anodization technique. In this method, Zn sheet acted as the anode and Pb sheet served as the counter electrode, and the complex solution of HF-C2H5OH-H2O was used as electrolyte. ZnO nanowires were characterized by Field Emission Scanning Electron Microscopy (FE-SEM), Transmission Electron Microscopy (TEM) and Selected Area Electron Diffraction (SAED) and X-ray Diffraction (XRD). The results show that the nanowires were wurtzite crystalline ZnO, and the ZnO nanowires with the diameters of 70 nm and 30～40 nm were obtained by adjusting preparation conditions, respectively.
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| 关 键 词： | ZnO纳米线 电化学 阳极氧化 制备 |
| 文章编号： | 1001-4861(2005)04-0583-05 |
| 收稿时间： | 2004/8/10 0:00:00 |
| 修稿时间： | 2004年8月10日 |
Preparation of ZnO Nanowires by Electrochemical Method |
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| MENG A-Lan,LIN Yu-Sheng and WANG Guang-Xin.Preparation of ZnO Nanowires by Electrochemical Method[J].Chinese Journal of Inorganic Chemistry,2005,21(4):583-587. |
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| Authors: | MENG A-Lan LIN Yu-Sheng and WANG Guang-Xin |
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| Institution: | College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042,College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042 and College of Chemistry and Molecular Engineering, Qingdao University of Science and Technology, Qingdao 266042 |
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| Abstract: | High-quality ZnO nanowires have been synthesized at relatively low temperature via one-step electrochemical anodization technique. In this method, Zn sheet acted as the anode and Pb sheet served as the counter electrode, and the complex solution of HF-C2H5OH-H2O was used as electrolyte. ZnO nanowires were characterized by Field Emission Scanning Electron Microscopy (FE-SEM), Transmission Electron Microscopy (TEM) and Selected Area Electron Diffraction (SAED) and X-ray Diffraction (XRD). The results show that the nanowires were wurtzite crystalline ZnO, and the ZnO nanowires with the diameters of 70 nm and 30~40 nm were obtained by adjusting preparation conditions, respectively. |
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| Keywords: | ZnO nanowires electrochemical anodization synthesize |
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