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| A NOVEL IRON—SULFUR—THIOLATE BASKET CLUSTER：CRYSTAL STRUCTURE OF Fe6S5（μ—SPh）（P—n—Bu3）4（SPh）2 | |
| 引用本文： | 蔡进华,陈昌能,等. A NOVEL IRON—SULFUR—THIOLATE BASKET CLUSTER：CRYSTAL STRUCTURE OF Fe6S5（μ—SPh）（P—n—Bu3）4（SPh）2[J]. 结构化学, 1989, 8(3): 220-224 |
| 作者姓名： | 蔡进华 陈昌能 等 |
| 摘 要： | <正> Fe6S5 (u-SPh) (P-n-Bu3)A (SPh )2, Mr = 1632. 21 , triclinic, P1, a = 11.877(3), b=14. 302(3), c= 24. 920(2) A ,a= 94. 84 (2), B = 96. 59 (2), y = 100. 44(2),V= 4111.7(13)A3,Z=2,Dx==1. 32gcm3,MoKa(0. 71069A),u=13.4 cm-1,F(000) = 1726,T=293K,R(Ru) = 0. 077(0. 060) for 6042 observed (I>3o(I)) reflections. |
| 关 键 词： | 晶体结构 铁 硫酚 原子簇合物 |
A NOVEL IRON SULFUR THIOLATE BASKET CLUSTER:CRYSTAL STRUCTURE OF Fe_6S_5 (μ-SPh) (P-n-Bu_3)_4(SPh)_2 |
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| Abstract: | Fe6S5 (u-SPh) (P-n-Bu3)A (SPh )2, Mr = 1632. 21 , triclinic, P1, a = 11.877(3), b=14. 302(3), c= 24. 920(2) A ,a= 94. 84 (2), B = 96. 59 (2), y = 100. 44(2),V= 4111.7(13)A3,Z=2,Dx==1. 32gcm3,MoKa(0. 71069A),u=13.4 cm-1,F(000) = 1726,T=293K,R(Ru) = 0. 077(0. 060) for 6042 observed (I>3o(I)) reflections. |
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