Thermal analysis applied in the crystallization study of SrSnO3 |
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| Authors: | Mary C F Alves Soraia C Souza Márcia R S Silva Elaine C Paris S J G Lima R M Gomes E Longo A G de Souza and Iêda M Garcia dos Santos |
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| Institution: | (1) LACOM, Departamento de Qu?mica/CCEN, Universidade Federal da Para?ba, Campus I, Jo?o Pessoa, PB, Brazil;(2) LSR, Departamento de Engenharia Mec?nica/CT, UFPB, Campus I, Jo?o Pessoa, PB, 58059-900, Brazil;(3) CMDMC—LIEC, Instituto de Qu?mica, UNESP, Araraquara, SP, Brazil; |
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| Abstract: | SrSnO3 was synthesized by the polymeric precursor method with elimination of carbon in oxygen atmosphere at 250 °C for 24 h. The
powder precursors were characterized by TG/DTA and high temperature X-ray diffraction (HTXRD). After calcination at 500, 600
and 700 °C for 2 h, samples were evaluated by X-ray diffraction (XRD), infrared spectroscopy (IR) and Rietveld refinement
of the XRD patterns for samples calcined at 900, 1,000 and 1,100 °C. During thermal treatment of the powder precursor ester
combustion was followed by carbonate decomposition and perovskite crystallization. No phase transition was observed as usually
presented in literature for SrSnO3 that had only a rearrangement of SnO6 polyhedra. |
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